A Practical Method for O-Acylation of N-Hydroxythiazole-2(3H)-thiones
SYNTHESIS-STUTTGART. H. 3. 2010 S. 538 - 542
Erscheinungsjahr: 2010
ISBN/ISSN: 0039-7881
Publikationstyp: Zeitschriftenaufsatz
Doi/URN: 10.1055/s-0029-1217102
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Inhaltszusammenfassung
O-Acylation of 4-and 4,5-substituted N-hydroxythiazole-2(3H)-thiones occurred in solutions of acetone upon treatment with solid K2CO3 and a variety of neat acyl chlorides (primary, secondary, and tertiary alkyl, aryl; 60-87% yield; similar to 10 g scale).
